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E-grāmata: Chemical Food Contaminants Analysis

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Chemical Food Contaminants AnalysisPalielināt
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This volume provides protocols on different combinations of contaminates, matrices, and sample preparation. Chapters are divided into two parts, detailing polycyclic aromatic hydrocarbon,dioxins, furans, organochlorie pesticides, toxic elements, mycotoxins, mercury in food products, acrylamine, polypeptide antibiotics, tetracyclines, coccidiostats, beta-blockers, sedatives,glucocorticoids, palytoxin-like marine biotoxins in fish, polar drugs and contaminants in animal feed, UV filters, micro and nanoplastics in seafood, tetracyclines in vegetables, MCPDEs, and pharmaceuticals in seafood. Written in the format of the Methods and Protocols in Food Science (MeFS) series, the chapters include an introduction to the respective topic, list necessary materials and reagents, detail well-established and validated methods for readilyreproducible laboratory protocols, and contain notes on how to avoid or solve typical problems.









 Authoritative and cutting-edge,Chemical Food Contaminants Analysis aims to ensure successful results in the further study of this vital field
Determination of polycyclic aromatic hydrocarbons (PAHs) in seafood by
matrix solid-phase dispersion and pressurized liquid extraction followed by
GC-MS/MS analysis.- Determination of polychlorinated dibenzo-p-dioxins
(PCDDs), polychlorinated dibenzofurans (PCDFs), and dioxin-like
polychlorinated biphenyls (dl-PCBs) in food by GC-MS/MS.- Simultaneous
analysis of polychlorinated biphenyls (PCBs) and organochlorine pesticides
(OCPs) in animal fat by GC-ECD and GC-MS.- Determination of As, Cd, Hg and Pb
in milk, meat, rice, and garlic by ICP-MS.- Determination of sedatives and
-blockers residues in bovine, swine, and equine kidney by liquid
chromatography coupled to tandem mass spectrometry.- Determination of
pesticides and mycotoxins in malt, brewers spent grain, and beer using a
dilute-and-shoot procedure and HPLC-MS/MS.- Screening of antimicrobials
residues in muscle from different species by liquid chromatography coupled
with tandem mass spectrometry.- Determination of ochratoxin A in plant
products: immunoaffinity column and liquid chromatography with fluorescence
detector.- Total mercury determination in fish muscle: direct analysis by
atomic absorption spectrophotometer.- Determination of polypeptide
antibiotics in milk by simple LLE technique and LCMS/MS
analysis.- Determination of tetracyclines and their 4-epimers in milk by
solid-phase extraction (SPE) and liquid chromatography tandem mass
spectrometry.- Optimization of heavy metal tracing by total reflection x-ray
fluorescence: the experts' tips.- Determination of acrylamide in sweet potato
products using QuEChERS sample preparation followed by LC-ESI-MS/MS
analysis.- Determination of p-nitroaniline residues in chicken meat by
salting-out liquid-liquid extraction (SALLE) followed by derivatization and
LC-MS/MS analysis.- Determination of glucocorticoid residues in bovine,
swine, and equine liver by liquid chromatography coupledto tandem mass
spectrometry.- Screening of contaminants of emerging concern (CECs) in fish
and milk samples by liquid chromatography coupled with high-resolution tandem
mass spectrometry (LC-HRMS/MS).- Determination of N-nitro-, C-nitro-, and
C-nitrous-type compounds in meat products by d-SPE extraction and liquid
chromatography coupled to mass spectrometry.- Determination of polar
veterinary drugs and melamine in feeds: method using  ion-pair reversed-phase
or hydrophilic interaction liquid chromatography coupled to tandem mass
spectrometry.- Miniaturized extraction method based on bead beating
tissuelyser for the analysis of pharmaceuticals in seafood.- Determination of
UV filters and metabolites in seafood by HPLC-MS/MS.- Determination of
palytoxins oxidation products in seafood using solid phase extraction and
liquid chromatography-tandem mass spectrometry.- A rapid method for screening
microplastic in seafood using NileRed (NR) and fluorescence preceding
spectroscopic polymer analysis.- Determination of pyrrolizidine alkaloids in
plants, pollen, and honey by LC-ESI-MS/MS.- Conventional and dispersive solid
phase extraction clean-up approaches for the simultaneous analysis of
tetracyclines and sulfonamides in a variety of fresh
vegetables.- Determination of 2-monochloropropane-1,3-diol esters (2-MCPDE),
3-monochloropropane-1,2-diol esters (3-MCPDE) and glycidyl esters (GE) in
marine oil-based supplement by acid transesterification via gas
chromatography coupled to mass spectrometry (GC-MS).
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