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E-grāmata: Chromatography and Separation Science

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(President, Ahuja Consulting for Water Quality, Calabash, NC, USA)
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Chromatography and Separation SciencePalielināt
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The basic objectives of this book are to: provide basic information on chromatography and separation science; show how simple extraction and partition processes provide the basis for development of chromatography and separation science; describe the role of chromatography and separation science in various fields; discuss the role of chromatography and separation science in development of new methodology; and present new evolving methods and how to select an optimum method.

· The book covers the fundamental physical and chemical phenomena involved in separations
· Provides a concise overview of the basics of transport phenomena and thermodynamics
· Shows the importance of chromatography within separation science

Papildus informācija

The book covers the fundamental physical and chemical phenomena involved in separations Provides a concise overview of the basics of transport phenomena and thermodynamics Shows the importance of chromatography within separation science
Preface ix
Relating Chromatography to Separations
Defining Separation
2(1)
Evolution of Chromatography
3(3)
Separations in Everyday Life
6(1)
Basis of Separations
7(6)
Modes of Chromatography
13(1)
Unified Separation Science
14(1)
Selectivity and Detectability
15(3)
References
16(1)
Questions for Review
16(2)
Simple Separation Methods
Evaporation
18(1)
Precipitation
18(1)
Crystallization
19(1)
Filtration
19(2)
Membrane Separations
21(3)
Distillation
24(2)
Extraction
26(12)
References
35(1)
Questions for Review
35(3)
Equilibrium Processes in Separations
Molecular Interactions
38(1)
Separation Thermodynamics
38(11)
References
48(1)
Questions for Review
48(1)
The Molecular Basis of Separation
Molecular Interactions
49(11)
Solubility Parameter Theory
60(5)
Group Interactions
65(5)
References
67(1)
Questions for Review
67(3)
Mass Transport and Separation
Types of Diffusion
70(1)
Modeling Diffusion
71(1)
Chromatographic Implications
72(2)
Diffusion Rates in Various Media
74(3)
Mass Transfer
77(7)
References
79(1)
Questions for Review
79(5)
Chromatographic Methods
General Classification of Chromatographic Methods
84(3)
Classification Based on Retention Mode
87(3)
Classification Based on Sample Introduction
90(3)
Separation Characteristics of Chromatographic Methods
93(2)
Basic Chromatographic Theory
95(7)
References
99(1)
Questions for Review
100(2)
Paper Chromatography
Chromatography Paper
102(1)
Sample Preparation
103(1)
Sample Cleanup
104(1)
Derivatization
105(1)
Mobile Phases and Stationary Phases
106(4)
Development of Chromatograms
110(1)
Detection
111(1)
Quantitation
112(2)
References
112(1)
Questions for Review
112(2)
Thin-Layer Chromatography
Stationary Phases for TLC
114(3)
TLC of Enantiomeric Compounds
117(2)
Sample Application
119(4)
Mobile Phases
123(1)
Development of Chromatograms
124(1)
Detection and Quantitation
125(1)
Applications
126(8)
References
131(1)
Questions for Review
131(3)
Gas Chromatography
Equipment
134(1)
Separation Process
135(1)
Columns
136(6)
Gas Chromatographic Detectors
142(3)
Recording and Analysis
145(1)
Resolution
146(1)
Selection of a Stationary Phase
147(7)
References
152(1)
Questions for Review
152(2)
High-Pressure Liquid Chromatography
Evolution of HPLC
154(1)
Advantages over Gas Chromatography (GC)
155(2)
Separation Process
157(3)
Retention Parameters in HPLC
160(3)
Resolution and Retention Time
163(4)
Equipment
167(1)
Separation Mechanism in HPLC
168(11)
Stationary Phase Effects
179(1)
A Case Study of Retention Mechanism Investigations
180(2)
Molecular Probes/Retention Index
182(3)
Mobile Phase Selection and Optimization
185(26)
References
205(3)
Questions for Review
208(3)
Evolving Methods and Method Selection
Evolving Methodologies
211(9)
Selection of a Separation Method
220(3)
Chiral Separations
223(16)
Comparison of GC, SFC, HPLC, and CEC for a Selective Separation
239(4)
References
240(1)
Questions for Review
241(2)
Index 243


Satinder Ahuja is a leading expert on water quality improvement. He earned his PhD in analytical chemistry from the University of the Sciences in Philadelphia. He worked for Novartis Corp. in various leadership positions for over 25 years and taught as an adjunct professor at Pace University for over 10 years. As president of Ahuja Consulting, he advises on water quality issues relating to chemicals and pharmaceuticals. A member of the executive committee of the Rivers of the World Foundation (ROW), Dr. Ahuja has organized numerous global symposia on improving water quality, including presentations for the American Chemical Society and UNESCO. Dr. Ahuja has published numerous papers and more than 25 books. His latest books are Contaminants in Our Water (ACS, 2020); Evaluating Water Quality to Prevent Future Disasters (Elsevier, 2019); Advances in Water Purification Techniques (Elsevier, 2019); and Chemistry and Water (Elsevier, 2017).
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