| Preface |
|
| Laboratory Safety Rules |
|
1 | (6) |
| Introduction |
|
7 | (1) |
|
Evaluation of Experimental Data |
|
|
7 | (3) |
|
The Use of the Laboratory Balance |
|
|
10 | (1) |
|
|
|
10 | (1) |
|
|
|
11 | (1) |
|
|
|
12 | (1) |
|
Sample Laboratory Experiment Report |
|
|
13 | (4) |
|
|
|
17 | (8) |
|
Formula and Composition of a Hydrate |
|
|
25 | (6) |
|
Physical Changes and Chemical Reactions |
|
|
31 | (10) |
|
Types of Chemical Reactions |
|
|
41 | (10) |
|
The Stoichiometry of a Reaction |
|
|
51 | (6) |
|
Identification of Common Chemicals |
|
|
57 | (8) |
|
Titration of Acids and Bases |
|
|
65 | (6) |
|
Gravimetric and Volumetric Analysis |
|
|
71 | (8) |
|
|
|
79 | (10) |
|
Evaluation of the Gas Law Constant |
|
|
89 | (6) |
|
Thermochemistry: The Heat of Reaction |
|
|
95 | (12) |
|
Spectrophotometric Analysis of Commercial Aspirin |
|
|
107 | (12) |
|
Molecular Models and Covalent Bonding |
|
|
119 | (8) |
|
LeChatelier's Principle in Iron Thiocyanate Equilibrium |
|
|
127 | (6) |
|
A Kinetic Study of an Iodine Clock Reaction |
|
|
133 | (8) |
|
Determination of an Equilibrium Constant |
|
|
141 | (8) |
|
Determination of Iron in Vitamins |
|
|
149 | (8) |
|
Weak Acids and Bases and Their Salts |
|
|
157 | (12) |
|
Determination of the Ionization Constant of a Weak Acid |
|
|
169 | (10) |
|
Investigation of Buffer Systems |
|
|
179 | (8) |
|
Determination of Acid-Neutralizing Power of Commercial Antacids |
|
|
187 | (6) |
|
Determination of a Solubility Product Constant |
|
|
193 | (10) |
|
Oxidation-Reduction Titration |
|
|
203 | (6) |
|
Electrolysis: Faraday's Law and Determination of Avogadro's Number |
|
|
209 | (8) |
|
An Investigation of Voltaic Cells - The Nernst Equation |
|
|
217 | (10) |
|
Determination of Water Hardness |
|
|
227 | (8) |
|
The Solvay Process: Preparation of NaHCO3 and Na2CO3 |
|
|
235 | (6) |
|
A Penny's Worth of Chemistry |
|
|
241 | (10) |
|
|
|
251 | (6) |
|
Preparation of [ Co(NH3)5ONO]Cl2 - Linkage Isomerism |
|
|
257 | (6) |
|
Free Radical Bromination of Organic Compounds |
|
|
263 | (6) |
|
Paper Chromatography: Separation of Amino Acids |
|
|
269 | (22) |
|
Introduction to Qualitative Analysis (Experiments 33 - 38) |
|
|
281 | (1) |
|
The Basis for the Organization of the Analytical Scheme |
|
|
281 | (1) |
|
|
|
282 | (1) |
|
Laboratory Techniques for Qualitative Analysis |
|
|
283 | (3) |
|
|
|
286 | (1) |
|
|
|
286 | (5) |
|
|
|
291 | (4) |
|
|
|
295 | (4) |
|
The Hydrogen Sulfide Group |
|
|
299 | (10) |
|
The Ammonium Sulfide Group |
|
|
309 | (10) |
|
|
|
319 | (6) |
|
Analysis of Common Anions and Their Salts |
|
|
325 | (10) |
| Appendix |
|
|
I. The International System of Units (SI) |
|
|
333 | (1) |
|
II. Fundamental Constants and Conversions |
|
|
334 | (1) |
|
III. Common Conversion Factors |
|
|
334 | (1) |
| Qualitative Analysis Report Forms |
|
335 | |
