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Fundamentals of Environmental Sampling and Analysis, 2e Set 2nd edition [Hardback]

(University of Houston-Clear Lake)
  • Formāts: Hardback, height x width x depth: 259x183x46 mm, weight: 1678 g
  • Izdošanas datums: 03-Oct-2024
  • Izdevniecība: John Wiley & Sons Inc
  • ISBN-10: 1394244622
  • ISBN-13: 9781394244621
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Fundamentals of Environmental Sampling and Analysis, 2e Set 2nd editionPalielināt
  • Formāts: Hardback, height x width x depth: 259x183x46 mm, weight: 1678 g
  • Izdošanas datums: 03-Oct-2024
  • Izdevniecība: John Wiley & Sons Inc
  • ISBN-10: 1394244622
  • ISBN-13: 9781394244621
Citas grāmatas par šo tēmu:
Permanent link: https://www.kriso.lv/db/9781394244621.html
Keywords:

This book introduces a comprehensive overview on the fundamentals and applications of environmental sampling and analysis for students in environmental science and engineering as well as environmental professionals involved in sampling and analytical work.

The book details fundamentals of sampling, selection of standard methods, QA/QC, sample preparation, chemical and instrumental principles, and method applications to various contaminants in environmental matrices (air, water, soil, waste, and biological samples). The book gives an integrated introduction to sampling and analysis – both are essential to quality environmental data. For example, contrary to other books that introduce a specific area of sampling and analysis, this text provides a balanced mix of field sampling and laboratory analysis, essential knowledge in chemistry/statistics/hydrology/regulations, wet chemical methods for conventional chemicals as well as various modern instrumental techniques for contaminants of emerging concerns. The new edition adds three standalone chapters regarding the basics of analytical and organic chemistry, environmental data analysis, mass spectrometry and other significant amounts of new materials such as time-integrated passive sampling, incremental sampling, green sample preparation, Raman spectroscopy, chiral separation, and non-target analysis. In addition, the second edition provides more examples, visual aids, case studies, and end-of-chapter exercise problems to enhance a better understanding of the fundamentals of environmental sampling and analysis while incorporating current literature (mostly peer-reviewed journal papers) regarding the applications and challenges in the field of environmental sampling and analysis.

Fundamentals of Environmental Sampling and Analysis, 2nd Edition TOC:

List of Case Studies xiii

List of Boxes xiv

Preface xvi

New in the Second Edition xviii

About the Author xxi

Whom This Book Is Written For xxii

To the Instructor xxiii

Acknowledgments xxiv

List of Symbols xxvi

1 Introduction to Environmental Data Acquisition 1

1.1 Introduction 2

1.2 Environmental Sampling 9

1.3 Environmental Analysis 9

Chapter Themes 13

References 13

Questions 14

Problems 15

2 Basics of Analytical and Organic Chemistry 16

2.1 Basic Concepts from Analytical Chemistry 17

2.2 Basic Concepts from Organic Chemistry 27

Chapter Themes 47

References 48

Questions 49

Problems 51

3 Basics of Environmental Data Validation and Analysis 55

3.1 Measurements of Central Tendency and Dispersion 56

3.2 Understanding Probability Distributions 59

3.3 Hypothesis Testing and Type I and II Errors 65

3.4 Detection of Outliers 67

3.5 Analysis of Censored Data 72

3.6 Analysis of Spatial and Time Series Data 77

Chapter Themes 80

References 81

Questions 82

Problems 83

4 Environmental Sampling Design 87

4.1 Planning and Sampling Protocols 88

4.2 Sampling Environmental Population 91

4.3 Environmental Sampling Approaches: Where and When 95

4.4 Estimating Sample Numbers and Sampling Frequencies 108

Chapter Themes 112

References 113

Questions 115

Problems 116

5 Environmental Sampling Techniques 120

5.1 General Guidelines of Environmental Sampling Techniques 121

5.2 Grab Sampling Techniques for Various Media: Practical Approaches and
Tips 136

5.3 Time-Integrated Sampling and Sensing Techniques 148

Chapter Themes 153

References 154

Questions 156

Problems 158

6 Methodology and Quality Assurance/Quality Control of Environmental
Analysis 159

6.1 Overview on Standard Methodologies 160

6.2 Selection of Standard Methods 169

6.3 Field Quality Assurance/Quality Control 175

6.4 Analytical Quality Assurance/Quality Control 177

Chapter Themes 185

References 186

Questions 187

Problems 189

7 Wet Chemical and Field Methods for Common Environmental Parameters 191

7.1 Basic Operations in Environmental Laboratories 192

7.2 Wet Chemical Methods and Common Techniques in Environmental Analysis
200

7.3 Analytical Principles for Common Wet Chemical Methods 204

7.4 Field Monitoring Testing Kits and Sensors 221

Chapter Themes 224

References 224

Questions 225

Problems 226

8 Fundamentals of Sample Preparation for Environmental Analysis 229

8.1 Overview of Sample Preparation 230

8.2 Sample Preparation for Metal Analysis 233

8.3 Extraction for SVOC and Non-VOC from Liquid or Solid Samples 240

8.4 Sample Preparation for VOC in Liquid and Solid Samples 251

8.5 Post-Extraction Cleanup of Organic Compounds 255

8.6 Derivatization for GC and HPLC Analysis 257

Chapter Themes 260

References 260

Questions 262

Problems 263

9 Molecular Spectroscopic Methods in Environmental Analysis 264

9.1 An Introduction to Molecular Spectroscopy 265

9.2 UV-Visible Spectroscopy 271

9.3 Infrared Spectroscopy 286

9.4 Raman Spectrometry 296

9.5 Photoluminescence and Chemiluminescence 299

Chapter Themes 300

References 301

Questions 302

Problems 305

10 Atomic Spectroscopy for Metal Analysis 306

10.1 Introduction to the Principles of Atomic Spectroscopy 307

10.2 Instruments for Atomic Spectroscopy 313

10.3 Selection of the Proper Atomic Spectroscopic Techniques 320

10.4 Speciation of Metals in Environmental Samples 325

10.5 Practical Tips to Metal Analysis 326

Chapter Themes 331

References 332

Questions 333

Problems 335

11 Chromatographic Methods for Environmental Analysis 336

11.1 Introduction to Chromatography 337

11.2 Instruments of Chromatographic Methods 356

11.3 Common Detectors for Chromatography 363

11.4 Applications of Chromatographic Methods in Environmental Analysis 371

11.5 Practical Tips to Chromatographic Methods 375

Chapter Themes 379

References 380

Questions 381

Problems 383

12 Electrochemical Methods for Environmental Analysis 385

12.1 Introduction to Electrochemical Theories 386

12.2 Potentiometric Applications in Environmental Analysis 395

12.3 Voltammetric Applications in Environmental Analysis 401

Chapter Themes 406

References 407

Questions 408

Problems 410

13 Mass Spectrometry in Environmental Analysis 411

13.1 Basics of Mass Spectrometry 412

13.2 Ionization Techniques 417

13.3 Mass Analyzers 428

13.4 Hyphenated Mass Spectrometric Methods 435

13.5 Mass Spectra and Molecule Fragmentation 442

13.6 Mass Spectrometric Applications in Environmental Analysis 448

Chapter Themes 451

References 452

Questions 453

Problems 458

14 Other Instrumental Methods in Environmental Analysis 459

14.1 Nuclear Magnetic Resonance (NMR) Spectroscopy 460

14.2 Surface and Microscopic Characterization 474

14.3 Radiochemical Analysis 484

14.4 Screening Methods Using Immunoassay 489

Chapter Themes 489

References 490

Questions 491

Problems 494

Appendix A: Common Abbreviations and Acronyms 495

Appendix B1: National Primary Drinking Water Regulations 503

Appendix B2: National Ambient Air Quality Standards 507

Appendix C: Structures and Properties of Important Organic Pollutants 508

Appendix D1: Standard Normal Cumulative Probabilities 519

Appendix D2: Percentiles of Students t Distribution 521

Appendix D3: Critical Values for the F-Distribution 523

Appendix E: Required Containers, Preservation Techniques, and Holding Times
526

Appendix F: Answers to Selected Questions and Problems 529

Appendix G: Periodic Table 537

Index 538

Fundamentals of Environmental Sampling and Analysis, 2nd Edition Solutions
Manual TOC:

Chapter 1 Questions 1

Problems 5

Chapter 2 Questions 6

Problems 12

Chapter 3 Questions 17

Problems 19

Chapter 4 Questions 33

Problems 39

Chapter 5 Questions 49

Problems 53

Chapter 6 Questions 56

Problems 63

Chapter 7 Questions 67

Problems 74

Chapter 8 Questions 79

Problems 87

Chapter 9 Questions 90

Problems 96

Chapter 10 Questions 100

Problems 108

Chapter 11 Questions 110

Problems 121

Chapter 12 Questions 124

Problems 131

Chapter 13 Questions 133

Problems 145

Chapter 14 Questions 147

Problems 160