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E-grāmata: Further Radiopharmaceuticals for Positron Emission Tomography and New Strategies for Their Production, Volume 2

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This book describes methods and procedures for preparing PET radiopharmaceuticals, and highlights new methods for conducting radiochemical reactions with carbon-11 (C11) and fluorine-18 (F18), which are two of the most commonly used radionuclides in positron emission tomography (PET) imaging.

    Provides reliable methods for radiochemical syntheses and reactions, including all essential information to duplicate the procedure     Eliminates the time-consuming process of searching journal articles and extracting pertinent details from lengthy experimental sections or supporting information     Focuses on an emerging and important area for pharmaceutical and medical applications     Encompasses technical, regulatory, and application aspects     Includes solid-phase radiochemistry, transition-metal catalyzed radiochemistry, microfluidics, click chemistry, green radiochemistry and new strategies for radiopharmaceutical quality control
Contributors xi
Editorial Preface xvii
Abbreviations xix
PART I FLUORINE-18 LABELED RADIOPHARMACEUTICALS
1(62)
1 Synthesis of (--)-[ 18F]Flubatine ([ 18F]FLBT)
3(10)
Megan N. Stewart
Brian G. Hockley
Peter J. H. Scott
2 Synthesis of [ 18F]-(--)Fluoroethoxy Benzovesamicol ([ 18F]FEOBV)
13(8)
Brian G. Hockley
Megan N. Stewart
Peter J. H. Scott
3 Synthesis of [ 18F]Fluoromethylcholine ([ 18F]FCH) via [ 18F]Fluoromethyl Tosylate
21(8)
Melissa E. Rodnick
Allen F. Brooks
Brian G. Hockley
Bradford D. Henderson
Peter J. H. Scott
4 Radiosynthesis of [ 18F]Flotegatide ([ 18F]RGD-K5)
29(12)
Hartmuth C. Kolb
Fanrong Mu
Umesh Gangadharmath
Vani P. Mocharla
Zhihong Zhu
Ashok Chaudhary
Joseph C. Walsh
5 Synthesis of 3-[ 18F]Fluoro-5-(2-Pyridinylethynyl) Benzonitrile ([ i8F]FPEB)
41(12)
Steven H. Liang
Daniel L. Yokell
Raul N. Jackson
Peter A. Rice
Eli Livni
David Alagille
Gilles Tamagnan
Thomas Lee Collier
Neil Vasdev
6 Radiosynthesis of 2'-Deoxy-2'-[ 18F]Fluoro-5-Methyl-1-β-D-Arabinofuranosyluracil ([ 18F]FMAU)
53(10)
Kai Chen
Peter S. Conti
PART II CARBON-11 LABELED RADIOPHARMACEUTICALS
63(40)
7 Synthesis of N-[ 11C]Methyl-4-Piperidinyl Propionate ([ 11C]PMP)
65(8)
Xia Shao
Peter J. H. Scott
8 Synthesis of 1-(2,4-Dichlorophenyl)-4-Cyano-5-(4-[ 11C]methoxyphenyl)-N-(Piperidin-1-yl)-1H-Pyrazole-3-Carboxamide ([ 11C]OMAR)
73(8)
Xia Shao
Keunsam Jang
Peter J. H. Scott
9 Synthesis of Carbon-11 Labeled (+)-4-Propyl-3,4,4a,5,6, 10b-Hexahydro-2H-Naphtho[ 1,2-b][ 1,4]Oxazin-9-Ol ([ 11C]-(+)-PHNO)
81(12)
Christophe Plisson
Joaquim Ramada-Magalhaes
Jan Passchier
10 Synthesis of (R)-[ N-Methyl-11C]PK11195
93(10)
Vitor H. Alves
Antero J. Abrunhosa
Miguel Castelo-Branco
PART III OTHER RADIOPHARMACEUTICALS
103(12)
11 Synthesis of Oxygen-15 Water ([ 15O]H2O)
105(10)
David W. Dick
G. Leonard Watkins
PART IV NEW METHODS FOR THE SYNTHESIS AND QUALITY CONTROL OF RADIOPHARMACEUTICALS
115(132)
12 Direct, Nucleophilic Radiosynthesis of [ 18F]Trifluoroethyl Tosylate
117(6)
Patrick J. Riss
Waqas Rafique
Franklin I. Aigbirhio
13 Synthesis of [ 18F]N-Methyl Lansoprazole via Generation of a [ 18F]Trifluoromethyl Group
123(6)
Allen F. Brooks
Melissa E. Rodnick
Garret M. Carpenter
Peter J. H. Scott
14 [ 18F]Fluorination of (Mesityl)(Aryl)Iodonium Salts
129(10)
Naoko Ichiishi
Allen F. Brooks
Joseph J. Topczewski
Melissa E. Rodnick
Melanie S. Sanford
Peter J. H. Scott
15 Pd(IV)-Mediated Fluorination of Arenes with [ l8F]F- for PET Imaging
139(10)
Nathan J. Schauer
Stephen M. Carlin
Hong Ren
Jacob M. Hooker
16 Silicon Fluoride Acceptors (SIFAs) for Peptide and Protein Labeling with 18F
149(14)
Ralf Schirrmacher
Alexey Kostikov
Carmen Wangler
Klaus Jurkschat
Vadim Bernard-Gauthier
Esther Schirrmacher
Bjorn Wangler
17 Solid Phase Synthesis of [ 18F]-2-Fluoro-2-Deoxy-d-Glucose: A Resin-Linker-Vector (RLV) Approach
163(14)
Lynda J. Brown
Imtiaz Khan
Harry J. Wadsworth
Alexander Jackson
Nianchun Ma
Nicolas Millot
Sue M. Champion
Denis R. Bouvet
Alex M. Gibson
Richard C. D. Brown
18 Production and Reaction of [ 11C]Carbon Disulfide for the Synthesis of [ 11C]Dithiocarbamates
177(8)
Philip W. Miller
19 One-Pot, Direct Incorporation of [ 11CO2] into Carbamates
185(12)
Christian K. Moseley
Jacob M. Hooker
20 Radiosynthesis of [ 11C]Carboxamides via Reaction of [ 11C]CO2 Captured by a Cu(I)-Based Catalyst System with Boronic Acid Ester Precursors
197(10)
Patrick J. Riss
Shuiyu Lu
Sanjay Telu
Franklin I. Aigbirhio
Victor W. Pike
21 Ethanol as a Solvent for Carbon-11 Radiochemistry
207(26)
Xia Shao
Maria V. Fawaz
Keunsam Jang
Peter J. H. Scott
22 Synthesis and Applications of [ 11C]Hydrogen Cyanide
233(8)
Xia Shao
Melissa E. Rodnick
Allen F. Brooks
Peter J. H. Scott
23 Determination of Radiochemical Purity and Radiochemical Identity of [ 13N]NH3 Using Thin Layer Chromatography
241(6)
Peter A. Rice
Daniel L. Yokell
Appendix 1 Supplier Information 247(6)
Index 253
Peter J. H. Scott is an Assistant Professor in the Department of Radiology at the University of Michigan Medical School (USA), Director of the University of Michigan PET Center (USA) and a member of the Interdepartmental Program in Medicinal Chemistry. Professor Scott edited Linker Strategies in Solid-Phase Organic Synthesis (also from Wiley) and is the series editor for both the Wiley Series on Radiochemical Syntheses and the Wiley Series on Solid Phase Organic Syntheses.
Biežāk uzdotie jautājumi par e-grāmatām Biežāk uzdotie jautājumi par e-grāmatām
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