Contributors |
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xiii | |
About the editor |
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xv | |
Preface |
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xvii | |
Acknowledgments |
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xix | |
1 Introduction to Drying |
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1 | (14) |
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1 | (1) |
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1.2 Fundamental principles of drying: the concept of simultaneous heat and mass transfer |
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2 | (7) |
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1.2.1 Heat transfer during the drying process |
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2 | (4) |
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1.2.1.1 Conduction drying |
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3 | (1) |
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1.2.1.2 Convection drying |
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4 | (1) |
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1.2.1.3 Radiation and dielectric drying |
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5 | (1) |
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1.2.2 Mass transfer during the drying process |
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6 | (3) |
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1.2.2.1 Diffusion mechanism |
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7 | (1) |
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1.2.2.2 Capillary mechanism |
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8 | (1) |
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9 | (1) |
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9 | (3) |
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1.4.1 Constant rate period |
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10 | (1) |
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1.4.2 Falling rate period |
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11 | (1) |
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1.5 Techniques for the drying of dairy products |
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12 | (1) |
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13 | (1) |
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13 | (2) |
2 Dried Dairy Products and their Trends in the Global Market |
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15 | (8) |
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15 | (1) |
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2.2 Milk powders and dried milk products |
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16 | (2) |
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2.2.1 Primary dairy powders |
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16 | (1) |
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2.2.2 Secondary dairy powders |
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16 | (2) |
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2.3 World market dynamics |
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18 | (3) |
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18 | (2) |
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18 | (2) |
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20 | (1) |
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20 | (1) |
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20 | (1) |
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20 | (3) |
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20 | (1) |
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21 | (1) |
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21 | (1) |
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21 | (1) |
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21 | (2) |
3 Techniques for the Preconcentration of Milk |
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23 | (20) |
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23 | (1) |
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3.2 Need for preconcentration |
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23 | (2) |
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24 | (1) |
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3.2.2 Whey powders and infant formula |
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24 | (1) |
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3.3 Concentration methods |
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25 | (1) |
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25 | (5) |
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25 | (5) |
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3.4.1.1 Single-effect recirculation evaporator |
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25 | (1) |
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3.4.1.2 Multiple-effect evaporator |
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26 | (1) |
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3.4.1.3 Falling-film evaporator |
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27 | (1) |
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28 | (2) |
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3.4.1.5 Horizontal tube evaporator |
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30 | (1) |
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3.4.1.6 Mechanical film evaporator |
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30 | (1) |
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3.4.1.7 Low-temperature evaporator |
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30 | (1) |
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30 | (7) |
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3.5.1 Freeze concentration |
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30 | (2) |
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3.5.2 Membrane separation techniques |
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32 | (12) |
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34 | (1) |
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35 | (2) |
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37 | (1) |
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37 | (1) |
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37 | (6) |
4 Drum Drying |
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43 | (14) |
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43 | (1) |
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44 | (2) |
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4.2.1 Effect of operating parameters on product quality and the capacity of the drum dryer |
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45 | (1) |
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46 | (3) |
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46 | (1) |
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47 | (1) |
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47 | (1) |
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48 | (1) |
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4.3.5 Enclosed-drum dryers |
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49 | (1) |
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4.4 Classification of the feeding method |
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49 | (2) |
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4.4.1 Single- and multiple-roll feed |
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49 | (1) |
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49 | (1) |
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49 | (1) |
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49 | (1) |
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50 | (1) |
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51 | (3) |
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4.5.1 Important operational conditions in the drum drying of milk |
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52 | (2) |
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4.6 Advantages and disadvantages of drum/roller drying |
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54 | (1) |
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54 | (1) |
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55 | (2) |
5 Spray Drying |
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57 | (38) |
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57 | (1) |
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5.2 Spray drying: principle of operation |
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57 | (17) |
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59 | (6) |
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60 | (2) |
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5.2.1.2 Pressure nozzle atomizers |
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62 | (1) |
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5.2.1.3 Twin-fluid atomizers |
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62 | (1) |
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5.2.1.4 Monodisperse droplet generators |
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63 | (2) |
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5.2.2 Droplet-drying air interaction and moisture evaporation |
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65 | (7) |
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5.2.3 Particle separation |
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72 | (2) |
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5.3 Characteristics of spray-dried dairy powders |
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74 | (3) |
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74 | (1) |
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5.3.2 Particle size and shape parameters |
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75 | (2) |
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5.4 Handling spray-drying processing problems |
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77 | (2) |
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77 | (2) |
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5.4.2 Thermal denaturation of proteins |
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79 | (1) |
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5.5 Applications of spray drying for the production of dried milk and milk products |
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79 | (5) |
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84 | (4) |
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88 | (7) |
6 Freeze Drying |
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95 | (28) |
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95 | (1) |
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6.2 Steps in freeze drying |
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95 | (5) |
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96 | (3) |
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6.2.2 Primary or sublimation drying |
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99 | (1) |
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6.2.3 Secondary or desorption drying |
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100 | (1) |
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6.3 Merits of freeze drying over other drying techniques |
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100 | (1) |
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6.4 Heat and mass transfer in freeze drying |
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101 | (2) |
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6.5 Freeze-drying equipment |
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103 | (3) |
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6.6 Properties influencing the freeze drying of dairy products |
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106 | (5) |
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106 | (3) |
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109 | (2) |
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6.7 Preservation of kefir culture by freeze drying |
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111 | (1) |
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6.8 Microencapsulation of probiotics by freeze drying |
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112 | (3) |
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112 | (1) |
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6.8.2 Need for microencapsulation |
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113 | (1) |
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6.8.3 Cell viability issues associated with freeze drying |
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113 | (1) |
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6.8.4 Characteristics of microencapsulated probiotic cells |
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114 | (1) |
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115 | (2) |
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117 | (6) |
7 Spray Freeze Drying |
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123 | (26) |
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123 | (1) |
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124 | (8) |
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125 | (1) |
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126 | (4) |
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7.2.2.1 Spray freezing into vapour |
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127 | (1) |
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7.2.2.2 Spray freezing into vapour over liquid |
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127 | (2) |
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7.2.2.3 Spray freezing into liquid |
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129 | (1) |
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130 | (2) |
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7.2.3.1 Vacuum freeze drying |
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130 | (1) |
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7.2.3.2 Atmospheric SFD and atmospheric spray fluidized-bed freeze drying |
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131 | (1) |
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7.2.3.3 Sub-atmospheric pressure SFD |
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132 | (1) |
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7.3 Applications of SFD in dried dairy products |
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132 | (12) |
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7.3.1 SFD of whole milk and skim milk |
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133 | (2) |
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7.3.2 SFD of whey protein |
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135 | (5) |
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7.3.3 SFD for microencapsulation of probiotics |
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140 | (4) |
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7.4 Advantages and limitations of SFD |
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144 | (1) |
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144 | (1) |
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144 | (5) |
8 Optimization of Dairy Product Drying Processes |
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149 | (30) |
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149 | (1) |
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8.2 Experimental design tools for process optimization |
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149 | (7) |
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8.2.1 Response surface methodology |
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149 | (2) |
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8.2.1.1 Advantages of RSM |
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151 | (1) |
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8.2.1.2 Limitations of RSM |
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151 | (1) |
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8.2.2 Artificial neural networks |
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151 | (3) |
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8.2.2.1 Feed-forward neural network |
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152 | (1) |
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8.2.2.2 Learning process of an ANN |
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153 | (1) |
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8.2.2.3 Optimization of process parameters |
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154 | (1) |
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8.2.3 Finite element and finite volume methods |
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154 | (2) |
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8.2.3.1 Finite element method |
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155 | (1) |
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8.2.3.2 Finite volume method |
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155 | (1) |
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8.3 Drying process variables and their influence on process and product quality |
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156 | (14) |
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157 | (1) |
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8.3.1.1 Heat and mass transfer |
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157 | (1) |
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158 | (3) |
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8.3.2.1 Exergy efficiency |
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160 | (1) |
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160 | (1) |
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161 | (8) |
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8.3.3.1 Temperature measurement |
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162 | (2) |
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8.3.3.2 Computational modelling |
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164 | (5) |
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8.3.4 Spray freeze drying |
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169 | (1) |
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170 | (1) |
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171 | (8) |
9 Computational Fluid Dynamics Modelling of the Dairy Drying Processes |
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179 | (24) |
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179 | (1) |
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179 | (10) |
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9.2.1 Spray-drying process |
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179 | (1) |
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9.2.2 Flow field simulation |
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180 | (3) |
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9.2.2.1 Steady or unsteady approach |
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181 | (1) |
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9.2.2.2 Turbulence modelling |
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182 | (1) |
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9.2.3 Discrete phase modelling |
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183 | (3) |
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9.2.4 Wall deposition and the particle build-up model |
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186 | (1) |
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9.2.5 Particle interaction |
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186 | (3) |
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9.2.6 Validation and issues of CFD simulation |
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189 | (1) |
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189 | (4) |
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9.3.1 Modelling of freeze drying |
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190 | (13) |
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9.3.1.1 Mass and heat-transfer modelling |
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190 | (1) |
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9.3.1.2 Primary drying modelling |
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191 | (1) |
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9.3.1.3 Secondary drying modelling |
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192 | (1) |
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193 | (3) |
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9.5 Conclusions and future scope |
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196 | (1) |
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196 | (7) |
10 Physicochemical and Sensory Properties of Dried Dairy Products |
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203 | (26) |
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F. Magdaline Eljeeva Emerald |
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203 | (1) |
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10.2 Milk Powder Manufacture |
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203 | (5) |
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205 | (1) |
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206 | (2) |
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208 | (1) |
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10.2.4 Spray freeze drying |
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208 | (1) |
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10.3 Properties of dairy powders as influenced by drying method |
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208 | (1) |
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209 | (9) |
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10.4.1 Morphology, particle size, shape and distribution |
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209 | (1) |
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210 | (3) |
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10.4.3 Reconstitution properties |
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213 | (3) |
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10.4.4 Agglomeration and instantization |
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216 | (1) |
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10.4.5 Flowability and stickiness |
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216 | (1) |
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10.4.6 Heat and coffee stability |
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217 | (1) |
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10.5 Chemical and sensory properties |
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218 | (2) |
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218 | (1) |
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10.5.2 Non-enzymatic browning |
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219 | (1) |
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10.5.3 Oxidation and chemical quality |
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219 | (1) |
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220 | (1) |
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10.6 Properties of special powders |
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220 | (3) |
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220 | (1) |
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10.6.2 Whey protein concentrates |
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221 | (1) |
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221 | (1) |
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222 | (1) |
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10.6.5 Infant milk powders |
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222 | (1) |
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223 | (1) |
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223 | (1) |
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223 | (6) |
11 Packaging of Dried Dairy Products |
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229 | (20) |
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229 | (1) |
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11.2 Dairy packaging trends |
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230 | (1) |
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11.3 Forms of packaging materials |
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231 | (3) |
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232 | (1) |
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232 | (1) |
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11.3.3 Stretch-wrap packaging |
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232 | (1) |
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232 | (1) |
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11.3.5 Bag-in-box packages |
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233 | (1) |
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233 | (1) |
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11.3.7 Paper-board containers |
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233 | (1) |
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11.4 Packaging of dried milk products |
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234 | (3) |
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11.4.1 Packaging of whole milk powder |
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235 | (1) |
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11.4.2 Packaging of non-fat dried milk powder |
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236 | (1) |
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11.5 Developments in packaging techniques |
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237 | (7) |
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11.5.1 Intelligent packaging |
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237 | (1) |
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238 | (2) |
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11.5.2.1 Migration mechanism in active packaging |
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239 | (1) |
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11.5.2.2 The use of scavengers (absorbers) to prevent lipid oxidation |
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239 | (1) |
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11.5.3 Nanotechnology in dairy packaging |
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240 | (10) |
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11.5.3.1 Bionanocomposites and their applications |
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241 | (1) |
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11.5.3.2 Modelling the barrier properties of polymer-clay nanocomposites |
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242 | (2) |
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244 | (1) |
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244 | (5) |
12 Recent Advances in the Drying of Dairy Products |
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249 | (20) |
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249 | (1) |
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12.2 Typical layout of a dairy spray-drying process |
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250 | (2) |
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12.2.1 Multistage drying process |
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250 | (1) |
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12.2.2 Some unique process layouts |
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251 | (1) |
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12.3 Advances in operating spray dryers |
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252 | (9) |
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12.3.1 Controlling the drying process |
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252 | (7) |
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12.3.1.1 Single droplet to dryer-wide prediction |
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252 | (7) |
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12.3.2 Controlling powder stickiness and deposition |
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259 | (2) |
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12.4 Advances in operating fluidized-bed dryers |
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261 | (2) |
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12.4.1 Controlling crystallization |
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261 | (1) |
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12.4.2 Controlling agglomeration |
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262 | (1) |
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263 | (1) |
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263 | (6) |
13 Industrial Scale Drying of Dairy Products |
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269 | (18) |
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269 | (1) |
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13.2 Process flow in a dairy drying plant |
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270 | (2) |
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13.3 Lexicon of industrial-scale drying |
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272 | (1) |
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13.4 Industrial spray drying of dairy products |
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273 | (6) |
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13.4.1 Automation of industrial-scale spray dryers |
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273 | (1) |
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13.4.2 Efficiency of spray-dryer operation |
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274 | (2) |
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13.4.3 Bottlenecks in industrial spray-drying |
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276 | (1) |
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13.4.4 Hygiene in spray-dryer operation |
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277 | (1) |
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13.4.5 Safety aspects of spray drying |
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278 | (1) |
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13.5 Industrial drum drying of dairy products |
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279 | (4) |
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13.5.1 Critical control points in industrial drum drying |
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280 | (2) |
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13.5.2 Energy efficiency of drum drying |
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282 | (1) |
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13.5.3 Safe operation of drum dryers |
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283 | (1) |
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283 | (1) |
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283 | (4) |
14 Challenges Involved in the Drying of Dairy Powders |
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287 | (14) |
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287 | (1) |
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14.2 Challenges in the drying of dairy powders |
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288 | (7) |
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288 | (3) |
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288 | (1) |
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14.2.1.2 Factors affecting fouling |
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289 | (2) |
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291 | (1) |
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14.2.3 Fires and explosions |
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292 | (1) |
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293 | (1) |
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14.2.5 Transport of powder |
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293 | (1) |
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14.2.6 Storage of dairy powders |
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294 | (1) |
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294 | (1) |
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14.2.8 Development of specialty dairy powders |
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294 | (1) |
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14.3 Use of modelling as a tool to solve some challenges |
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295 | (1) |
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296 | (1) |
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296 | (5) |
Index |
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301 | |