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E-grāmata: Iptycenes Chemistry: From Synthesis to Applications

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  • Formāts: PDF+DRM
  • Izdošanas datums: 02-Dec-2012
  • Izdevniecība: Springer-Verlag Berlin and Heidelberg GmbH & Co. K
  • Valoda: eng
  • ISBN-13: 9783642328886
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Iptycenes Chemistry: From Synthesis to ApplicationsPalielināt
  • Formāts: PDF+DRM
  • Izdošanas datums: 02-Dec-2012
  • Izdevniecība: Springer-Verlag Berlin and Heidelberg GmbH & Co. K
  • Valoda: eng
  • ISBN-13: 9783642328886
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Iptycenes Chemistry: From Synthesis to Applications provides a comprehensive overview of the development of iptycene chemistry in the past seventy years. This book covers: (1) the basic nomenclature and general properties of iptycenes and their derivatives; (2) the synthesis and functionalization reactions of triptycenes, pentiptycenes, higher iptycenes, heterotriptycenes, and homotriptycenes; (3) the methods for the preparation of iptycene-based polymers with different types; and (4) the applications of iptycenes and their derivatives in molecular machines, materials science, host-guest chemistry, self-assembly, coordination chemistry, physical organic chemistry, medicinal chemistry, and so on. Consequently, such a book is not only helpful to researchers working in iptycene chemistry, but can also facilitate future research in wide areas.

This book presents a comprehensive overview of iptycene chemistry, from properties to synthesis, from preparation to derivatives, to applications in materials science, coordination chemistry, physical organic chemistry, medicinal chemistry, and more.
Part I Introduction and Background
1 Introduction and Background
3(10)
1.1 Introduction
3(1)
1.2 Structure Properties
4(1)
1.3 Physical and Chemical Properties
5(1)
1.4 Spectral Properties
5(3)
1.5 Nomenclature
8(5)
References
9(4)
Part II Synthesis and Reactions of Iptycenes and Their Derivatives
2 Synthesis and Reactions of Triptycenes and Their Derivatives
13(66)
2.1 Synthesis of Triptycenes and Their Derivatives
13(14)
2.2 Synthesis of Triptycenequinones and Their Derivatives
27(7)
2.3 Reactions of Triptycenes and Their Derivatives
34(24)
2.3.1 Nitration and Amination
34(4)
2.3.2 Acylation
38(2)
2.3.3 Halogenation
40(1)
2.3.4 Oxidation
41(2)
2.3.5 Reduction
43(3)
2.3.6 Photochemical Reactions
46(9)
2.3.7 Other Reactions
55(3)
2.4 Synthesis of Extended Triptycene Derivatives
58(11)
2.5 Synthesis and Reactions of Homotriptycenes
69(10)
References
72(7)
3 Synthesis and Reactions of Pentiptycenes and Their Derivatives
79(30)
3.1 Synthesis of Pentiptycenes and Their Derivatives
79(8)
3.2 Reactions of Pentiptycenes and Their Derivatives
87(11)
3.3 Synthesis of Extended Pentiptycenes Derivatives
98(11)
References
106(3)
4 Synthesis and Reactions of Other Iptycenes and Their Derivatives
109(20)
4.1 Heptiptycene and Noniptycene
109(9)
4.2 Miscellaneous
118(11)
References
126(3)
5 Synthesis and Reactions of Heterotriptycenes and Their Derivatives
129(44)
5.1 The Bridgehead-Substituted Heterotriptycenes
129(16)
5.1.1 Derivatives of Nitrogen Group Elements
129(9)
5.1.2 Derivatives of Carbon Group Elements
138(4)
5.1.3 Other Bridging Atoms
142(3)
5.2 The Heterotriptycenes with Heterocycles
145(18)
5.2.1 Derivatives of Nitrogen-Containing Heterocycles
145(10)
5.2.2 Derivatives of Sulfur-Containing Heterocycles
155(8)
5.3 Miscellaneous Heterotriptycenes and Their Derivatives
163(10)
References
168(5)
6 Preparation of Iptycene-Containing Polymers and Oligomers
173(38)
6.1 Triptycene-Containing Polymers
173(13)
6.1.1 Triptycene-Containing Non-conjugated Polymers
173(9)
6.1.2 Triptycene-Containing Conjugated Polymers
182(4)
6.2 Pentiptycene-Containing Polymers
186(6)
6.3 Other Iptycene-Containing Polymers
192(4)
6.4 Poly(iptycenes)
196(4)
6.5 Iptycene-Based Oligomers
200(11)
References
205(6)
Part III Applications of Iptycenes and Their Derivatives
7 Iptycenes and Their Derivatives in Molecular Machines
211(20)
7.1 Molecular Gearings
211(9)
7.2 Molecular Brakes and Ratchets
220(3)
7.3 Molecular Wheelbarrows
223(1)
7.4 Molecular Compasses and Gyroscopes
224(2)
7.5 Miscellaneous
226(5)
References
227(4)
8 Iptycenes and Their Derivatives in Material Science
231(20)
8.1 Liquid Crystals
231(6)
8.2 Optical and Electronic Materials
237(5)
8.3 Porous Materials for Adsorption and Separation
242(9)
References
248(3)
9 Iptycenes and Their Derivatives in Host-Guest Chemistry
251(38)
9.1 Triptycene-Derived Crown Ethers
251(15)
9.1.1 Triptycene-Derived Cylindrical Macrotricyclic Polyethers
251(12)
9.1.2 Tweezer-Like Triptycene-Derived Crown Ethers
263(3)
9.2 Triptycene-Derived Calixarenes
266(7)
9.3 Triptycene-Derived Oxacalixarenes and Azacalixarenes
273(3)
9.4 Other Triptycene-Derived Macrocyclic Hosts
276(5)
9.5 Pentiptycene-Derived Hosts
281(8)
References
286(3)
10 Iptycenes and Their Derivatives in Molecular Self-Assembly
289(34)
10.1 Self-Assembly in Crystal
289(16)
10.2 Self-Assembly on Surface
305(4)
10.3 Self-Assembly in Solution
309(14)
References
320(3)
11 Iptycenes and Their Derivatives in Coordination Chemistry
323(30)
11.1 Triptycene-Based Ligands
323(3)
11.2 Substituted Triptycene-Based Ligands
326(27)
11.2.1 Selenium Substitution
326(5)
11.2.2 Germanium and Silicon Substitution
331(2)
11.2.3 Phosphorus Substitution
333(7)
11.2.4 Miscellaneous Substitutions
340(9)
References
349(4)
12 Iptycenes and Their Derivatives in Sensors
353(12)
12.1 Sensors Based on Iptycene-Containing Polymers
353(7)
12.2 Other Iptycene-Based Sensors
360(5)
References
363(2)
13 Iptycenes and Their Derivatives in Molecular Balances
365(8)
References
371(2)
14 Miscellaneous Applications of Iptycenes and Their Derivatives
373
14.1 Medicinal Chemistry
373(1)
14.2 Model for Jahn-Teller Systems
374(2)
14.3 Artificial Photosynthesis Models
376(2)
14.4 Preparation of Carbene
378
References
380
Chuan-Feng Chen received his Ph.D. degree from Nanjing University in 1994. After working as a postdoctoral fellow at Institute of Chemistry, Chinese Academy of Sciences (ICCAS) for two years, he became an associate professor at the same Institute in 1996. From 1998 to 2001, he worked as a visiting scientist at University of New Mexico, USA. Then, he was promoted to a full professor of ICCAS in 2001. In 2000, he was selected for Hundred Talents Program by CAS. In 2006, he was awarded National Science Fund of China for Distinguished Young Scholars. Professor Chen is the author of more than 170 scientific publications. His current research interests include supramolecular chemistry based on novel synthetic hosts, hydrogen-bond-mediated molecular assemblies, helical foldamer and helicene chemistry. Ying-Xian Ma received her B.S. degree in Chemistry from Nankai University in 2010. She is currently a Ph.D. candidate under the direction of Professor Chuan-Feng Chen at the Institute of Chemistry, Chinese Academy of Sciences. Her research focuses on the synthesis and applicaitons of iptycenes in host-guest chemistry.
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