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Uniting Electron Crystallography and Powder Diffraction 2012 ed. [Mīkstie vāki]

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The polycrystalline and nanocrystalline states play an increasingly important role in exploiting the properties of materials, encompassing applications as diverse as pharmaceuticals, catalysts, solar cells and energy storage. A knowledge of the three-dimensional atomic and molecular structure of materials is essential for understanding and controlling their properties, yet traditional single-crystal X-ray diffraction methods lose their power when only polycrystalline and nanocrystalline samples are available. It is here that powder diffraction and single-crystal electron diffraction techniques take over, substantially extending the range of applicability of the crystallographic principles of structure determination. 

This volume, a collection of teaching contributions presented at the Crystallographic Course in Erice in 2011, clearly describes the fundamentals and the state-of-the-art of powder diffraction and electron diffraction methods in materials characterisation, encompassing a diverse range of disciplines and materials stretching from archeometry to zeolites.   As such, it is a comprehensive and valuable resource for those wishing to gain an understanding of the broad applicability of these two rapidly developing fields.
Part I Powder Diffraction
1 Powder Diffraction: By Decades
3(12)
William I.F. David
2 Rietveld Refinement
15(12)
Peter W. Stephens
3 Structure Solution -- An Overview
27(8)
Lynne B. McCusker
Christian Baerlocher
4 Inorganic Materials
35(10)
Radovan Cerny
5 Organic Compounds
45(8)
Kenneth Shankland
6 Laboratory X-ray Powder Diffraction
53(12)
Pamela Whitfield
7 Synchrotron X-Ray Powder Diffraction
65(18)
Fabia Gozzo
8 Ultrafast Powder Diffraction
83(12)
Andy Fitch
Caroline Curfs
9 Taking It to Extremes -- Powder Diffraction Under Non-Ambient Conditions
95(10)
David I.A. Millar
Colin R. Pulham
10 Structure Solution by Charge Flipping
105(12)
Lukas Palatinus
11 Structure Solution: Global Optimisation Methods
117(8)
Kenneth Shankland
12 Proteins and Powders: Technical Developments
125(12)
Jonathan P. Wright
13 Proteins and Powders: An Overview
137(12)
Irene Margiolaki
14 Parametric Powder Diffraction
149(16)
William I.F. David
John S.O. Evans
15 Powder Diffraction + Computational Methods
165(8)
L'ubomir Smrcok
16 Information on Imperfections
173(10)
Matteo Leoni
17 Pair Distribution Function Technique: Principles and Methods
183(12)
Simon J.L. Billinge
18 Debye Analysis
195(12)
Yuri G. Andreev
19 Quantitative Phase Analysis
207(12)
Ian C. Madsen
Nicola V.Y. Scarlett
Nathan A.S. Webster
20 Quantifying Amorphous Phases
219(14)
Arnt Kern
Ian C. Madsen
Nicola V.Y. Scarlett
21 Quantitative Phase Analysis: Method Developments
233(10)
Luca Lutterotti
22 Texture -- An Overview
243(8)
Robert B. Von Dreele
23 The Future of Powder Diffraction Is 2-D
251(10)
R.E. Dinnebier
B. Hinrichsen
Part II Electron Crystallography
24 Electron Crystallography -- New Methods to Explore Structure and Properties of the Nano World
261(10)
Ute Kolb
25 Image Formation in the Electron Microscope
271(10)
Louisa Meshi
26 Models for Precession Electron Diffraction
281(12)
Laurence D. Marks
27 Structure Solution Using HRTEM
293(10)
Sven Hovmoller
28 Combination of X-ray Powder Diffraction, Electron Diffraction and HRTEM Data
303(12)
Christian Baerlocher
Lynne B. McCusker
29 Automated Electron Diffraction Tomography
315(12)
Ute Kolb
30 Automated Quantitative 3D Electron Diffraction Rotation Tomography
327(10)
Peter Oleynikov
31 Introduction to ADT/ADT3D
337(12)
Tatiana E. Gorelik
Sebastian Schlitt
Ute Kolb
32 Electrostatic Potential Determined from Electron Diffraction Data
349(10)
Anatoly Avilov
33 Domino Phase Retrieval Algorithm for Structure Solution
359(10)
F.N. Chukhovskii
34 LARBED: Exploring the Fourth Dimension in Electron Diffraction
369(12)
Christoph T. Koch
35 Shadow Imaging for Charge Distribution Analysis
381(8)
Yimei Zhu
Lijun Wu
36 Electron Diffraction of Protein 3D Nanocrystals
389(10)
Jan Pieter Abrahams
Dilyana Georgieva
Linhua Jiang
Igor Nederlof
37 Parallel-Beam Diffraction and Direct Imaging in an Aberration-Corrected STEM
399(10)
Ondrej L. Krivanek
38 Electron Diffraction of Commensurately and Incommensurately Modulated Materials
409(10)
Joke Hadermann
Artem M. Abakumov
39 Detection of Magnetic Circular Dichroism Using TEM and EELS
419(10)
Stefano Rubino
Jan Rusz
Peter Schattschneider
Index 429